GET SOME THEORY FROM THE BOOKS
Wet abrasive cutting stands out as the most suitable method for materialographic cutting due to its minimal impact on the specimen in relation to the processing time. This technique involves the use of a cut-off wheel comprising abrasive particles and a binder.
DURING THE PROCEDURE
RECOMMENDED
We recommend you to mount your samples the most convenient way, giving attention to the heat resistance of the sample material, although, if a mounting press is unavailable, cold mounting becomes the sole viable option. Conversely, with access to a mounting press, the selection of mounting material can be refined based on specific attributes.
A crucial factor to consider is the abrasion rate, which denotes the speed at which material is ground or polished away. Ideally, the chosen mounting material should closely match the abrasion rate of the sample material. It is essential to recognize that the abrasion rate differs from the hardness of the sample.
As for the resin needs, we recommend the use of Epoxy resin as Epoxies offer a robust mounting solution with high resistance to chemicals and abrasion. Although they typically require a longer setup time compared to other castable materials, they exhibit superior flow and minimal shrinkage properties. For mounting challenging samples, long-cure epoxies are employed, and they can be introduced into a vacuum environment to eliminate trapped air and address voids.
IN THE END
If necessary, calibrate the sample with a coarser grit to make sure flat surface is achieved. The workpiece should be perfectly flat.
In the grinding steps for Structural Steel 42CrM04, when dealing with a flat sample, the process commences with a 40 µm. In case the sample is not flat, a coarser grit should be initially employed to achieve a flat surface (54 µm).
It's important to note that the applied force during grinding depends on the diameter of the sample, and in this instance, the sample has a diameter of 30mm. Additionally, to prevent excessive damage to the sample, it is recommended to rotate the sample clockwise.
Pre-polishing is not neccessairy in this step for this material.
In the polishing steps for Construction Steel 42CrM04, the process initiates with a 9 µm abrasive. Subsequently, following the 9 µm, a 2 µm abrasive is employed. The applied force during polishing is contingent on the diameter of the sample, with the current sample having a diameter of 30mm. During the 9 µm abrasive phase, it is recommended to rotate the sample in a counter-clockwise direction to eliminate scratches from coarser grits. Conversely, for the 2 µm abrasive, a clockwise rotation is advised to prevent excessive damage to the sample. It is crucial that all scratches align in the same direction, and if not, repeating the preceding step becomes necessary.
1 5000g 10x
Finally, a suitable pad with a colloidal silica solution is utilized to clean and execute the last polishing step, providing a mirror-like finish to the Structural Steel 42CrM04 sample.
2 Colloidal Silica 10x